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Beilstein J. Org. Chem. 2019, 15, 2774–2781, doi:10.3762/bjoc.15.269
Graphical Abstract
Scheme 1: Conventional method of synthesis of thiazolidine-2,4-dione derivatives.
Scheme 2: [2 + 2 + 2] Cyclotrimerization of N-methylthiazolidinedione.
Scheme 3: Unexpected product 5b obtained in the attempted NH-protection of thiazolidinedione with (Boc)2O.
Figure 1: Comparison of 13C NMR values of 9 and 5b.
Scheme 4: [2 + 2 + 2] Cyclotrimerization of dipropargylthiazolidinediones with propargyl halides.
Scheme 5: Formation of sultine 13 from compound 8b followed by DA reaction.
Scheme 6: Dipropargylation of 2,4-thiazolidinedione derivatives.
Scheme 7: [2 + 2 + 2] Cycloaddition in the presence of Wilkinson’s catalyst.
Scheme 8: N-Ester derivative 18 hydrolysis to N-acid derivative 22.
Scheme 9: Synthesis of triazolo derivative 24 via click reaction.
Beilstein J. Org. Chem. 2016, 12, 406–412, doi:10.3762/bjoc.12.43
Scheme 1: Synthesis of 3-substituted phospholanes according to earlier data [14-17].
Scheme 2: Synthesis of 3-substituted phospholanes.
Scheme 3: Synthesis of 3-substituted phospholane oxides and sulfides.
Scheme 4: Synthesis of 3-substituted 7a–f and 2-substituted 8a–f phospholanes.
Scheme 5: Synthesis of bisphospholanes.
Scheme 6: Synthesis of bisphospholane-1,1'-oxides and bisphospholane-1,1'-sulfides.
Scheme 7: Synthesis of the molybdenum complex (3-hexyl(benzyl)-1-phenyl(methyl)phospholane)Mo(CO)5.
Scheme 8: Synthesis of molybdenum complexes (1,2(1,6)-bis(1-phenylphospholan-3-yl)ethane(hexane))Mo(CO)5.